11-ID-D: High-energy X-ray Diffraction & Small Angle Scattering
XSD
Environmental Science, Materials Science, Physics
Environmental Science, Materials Science, Physics
11-ID-D will offer a wide range of experimental approaches with the highest available flux. Two dimensional focusing will be available with adaptable energy resolution. A q-range from 0.01A-1 to 40A-1 will be covered. The photon energy will cover the entire range from 26 to 130 keV. A secondary detector for spectroscopic/ Compton imaging will expand the multimodal approaches.
Beamline Specifications
Source :
Monochromator Type : Multilayer + secondary mono
Energy Range : 30-130 keV
Resolution : 2 x 10-4
Flux : 1 x 1013 @65 keV
Beam Size Hxv :
Focused : .5µm x .5µm
Unfocused : .5mm x .5mm
Monochromator Type : Multilayer + secondary mono
Energy Range : 30-130 keV
Resolution : 2 x 10-4
Flux : 1 x 1013 @65 keV
Beam Size Hxv :
Focused : .5µm x .5µm
Unfocused : .5mm x .5mm
Quick Stats
Current Status
Construction
Construction
Access Mode
On-site
On-site
Special Capabilities
Combination of high-energy x-ray total scattering including the small angle regime
Combination of high-energy x-ray total scattering including the small angle regime
Beamline Contacts
Beamline Techniques
High-energy x-ray diffraction
X-ray total scattering, pair distribution function (PDF)
Grazing incidence diffraction
Endstations
Detectors
Pilatus 2M
Perkin Elmer XRD 1621 amorphous silicon detector
Varex 4343CT (150 micron pixel size)
Equipment
2D focusing (>0.5 um x 0.5 um)
Flowcell/Controlled Atmosphere (RT to 1000C)
Multiple-sample furnace (RT to 400C)
Vertical furnace for melts (RT to 1000C)
Oxford Cryostream 800+ (80K-500K operations)
Electrochemistry cells thru APS E-Chem Lab
Programmable Mass Flow Controllers
Residual Gas Analyzer (with advanced notice)
PI Hexapod
Additional Information
Additional Information
https://www.aps.anl.gov/Structural-Science
https://www.aps.anl.gov/Structural-Science
Software
Linux workstation running SPEC; EPICS;
QXRD and areaDetector for data acquisition
GSAS-II and xPDFsuite for data processing
pdfgetx2, and pdfgetx3
Beamline Controls and Data Acquisition
Linux workstation running SPEC; EPICS;
QXRD and areaDetector for data acquisition
GSAS-II and xPDFsuite for data processing
pdfgetx2, and pdfgetx3