11-ID-B: Total scattering and powder diffraction
XSD
Catalysis, Chemistry, Environmental Science, GeoScience, Materials Science
Catalysis, Chemistry, Environmental Science, GeoScience, Materials Science
11-ID-B is a dedicated total scattering beamline for pair-distribution-function (PDF) analysis and also offers high-energy x-ray powder diffraction at fixed energies of 59 and 87 keV. Variable temperature measurements are supported (including low- and high-temperature 80K to 1200K). A variety of gases are available for reaction based, in-situ chemistry experiments. Electrochemical experiments are routinely supported. The addition of 1D focusing lenses and a high precision hexapod enable Grazing Incidence X-ray scattering. Visible light Raman scattering can be available as secondary probe for suitable experiments.
Beamline Specifications
Source :
Monochromator Type : Si(311)
Energy Range : 59- keV
Resolution : 1 x 10-3
Flux : 2.3 x 1012 @59 keV
Beam Size Hxv :
Focused : 400µm x 2µm
Unfocused : .5mm x .5mm
Source :
Monochromator Type : Si(422)
Energy Range : 87- keV
Resolution : 1 x 10-3
Flux : 5 x 1011 @87 keV
Beam Size Hxv :
Focused : 400µm x 2µm
Unfocused : .5mm x .5mm
Monochromator Type : Si(311)
Energy Range : 59- keV
Resolution : 1 x 10-3
Flux : 2.3 x 1012 @59 keV
Beam Size Hxv :
Focused : 400µm x 2µm
Unfocused : .5mm x .5mm
Source :
Monochromator Type : Si(422)
Energy Range : 87- keV
Resolution : 1 x 10-3
Flux : 5 x 1011 @87 keV
Beam Size Hxv :
Focused : 400µm x 2µm
Unfocused : .5mm x .5mm
Quick Stats
Current Status
Operational/Accepting General Users
Operational/Accepting General Users
Access Mode
On-site Remote
On-site Remote
Beamline Contacts
Beamline Techniques
X-ray total scattering, pair distribution function (PDF)
High-energy x-ray diffraction
Grazing incidence diffraction
Endstations
11-ID-B
11-ID-B is a dedicated total scattering beamline for pair-distribution-function (PDF) analysis and also offers high-energy x-ray powder diffraction at fixed energies of 59 and 87 keV. Variable temperature measurements are supported (including low- and high-temperature 80K to 1200K). A variety of gases are available for reaction based, in-situ chemistry experiments. Electrochemical experiments are routinely supported. The addition of 1D focusing lenses and a high precision hexapod enable Grazing Incidence X-ray scattering. Visible light Raman scattering can be available as secondary probe for suitable experiments.
11-ID-B is a dedicated total scattering beamline for pair-distribution-function (PDF) analysis and also offers high-energy x-ray powder diffraction at fixed energies of 59 and 87 keV. Variable temperature measurements are supported (including low- and high-temperature 80K to 1200K). A variety of gases are available for reaction based, in-situ chemistry experiments. Electrochemical experiments are routinely supported. The addition of 1D focusing lenses and a high precision hexapod enable Grazing Incidence X-ray scattering. Visible light Raman scattering can be available as secondary probe for suitable experiments.
Detectors
Perkin Elmer XRD1621 amorphous silicon detector
Varex 4343CT (150 micron pixel size)
Pilatus optional
Equipment
Flowcell/Controlled Atmospheres (RT to 1000C)
Multi-sample furnace (RT to 400C)
Vertical furnace for melts (RT to 1000C)
Visible light Raman spectrometer
Oxford cryosystems cryostream 800 plus <BR>(80 K to 500 K operations)
Electrochemistry cells thru APS E-Chem Lab
Programmable Mass Flow Controllers
Residual Gas Analyzer (with advanced notice)
Ambient multi-sample holder with data collection automation (20-50 samples)
PI Hexapod
1D Focusing Lenses (2um x 400 um) @ either energy
Additional Information
Additional Information
https://www.aps.anl.gov/Structural-Science
https://www.aps.anl.gov/Structural-Science
Software
Linux workstation running SPEC software;
QXRD for data acquisition;
GSAS-II and xPDFsuite for data processing;
pdfgetX2, and pdfgetx3
Linux workstation running SPEC software;
QXRD for data acquisition;
GSAS-II and xPDFsuite for data processing;
pdfgetX2, and pdfgetx3
Beamline Controls and Data Acquisition
Linux workstation running SPEC software;
QXRD for data acquisition;
GSAS-II and xPDFsuite for data processing;
pdfgetX2, and pdfgetx3
Linux workstation running SPEC software;
QXRD for data acquisition;
GSAS-II and xPDFsuite for data processing;
pdfgetX2, and pdfgetx3