12-ID-B: SAXS/WAXS
XSD
Chemistry, Life Sciences, Materials Science, Physics, Polymer Science
Chemistry, Life Sciences, Materials Science, Physics, Polymer Science
The 12-ID-B beamline is dedicated to SAXS including simultaneous SAXS/WAXS, GISAXS, and time-resolved SAXS for both solids and solutions. The beamline is equipped with furnaces, oven, gas and liquid flow systems, Linkam stages, and home-made multisample heater. Horizontal and vertical mirrors with 2 sets of slits deliver photons higher than 1E12 in the size of beam about 200 (H) x 40(V) um^2. The beam size can be slitted down to the size of about 10x10 um^2 if needed.
Beamline Specifications
Source :
Monochromator Type : Side bounce
Energy Range : 7.9-14 keV
Resolution : 1 x 10-4
Flux : 1 x 1012 @12 keV
Beam Size Hxv :
Focused : 200µm x 40µm
Unfocused : 1.5mm x 1mm
Monochromator Type : Side bounce
Energy Range : 7.9-14 keV
Resolution : 1 x 10-4
Flux : 1 x 1012 @12 keV
Beam Size Hxv :
Focused : 200µm x 40µm
Unfocused : 1.5mm x 1mm
Quick Stats
Current Status
Operational/Accepting General Users
Operational/Accepting General Users
Access Mode
On-site Remote
On-site Remote
Special Capabilities
Continually variable q range under computer control and simultaneous SAXS and WAXS.
Continually variable q range under computer control and simultaneous SAXS and WAXS.
Beamline Contacts
Beamline Techniques
Small-angle x-ray scattering
Grazing incidence small-angle scattering
Wide-angle x-ray scattering
Grazing incidence diffraction
Endstations
B station
Novel SAXS/WAXS chamber allowing simultaneous SAXS/WAXS and GISAXS. GIWAXS should be available in 2015.
Novel SAXS/WAXS chamber allowing simultaneous SAXS/WAXS and GISAXS. GIWAXS should be available in 2015.
B station
High resolution small angle x-ray diffraction. Beamsize can be as small as 10um in vertical direction.
High resolution small angle x-ray diffraction. Beamsize can be as small as 10um in vertical direction.
Detectors
Eiger 9M- SAXS
Pilatus 300K - WAXS
Perkin Elmer 4kx4k detector
Equipment
Temperature controlled flow cell (on-site)
Linkam TMS600 Hotstage (on-site)
Liquid autosampler coupled with flowcell
Potentiostat
FPLC
Multi-capillary/bulk sample heater
Hamilton dispenser
Additional Information
Additional Information
https://www.aps.anl.gov/Sector-12/12-ID-B
https://www.aps.anl.gov/Sector-12/12-ID-B
Software
12-ID-B uses Linux workstation running SPEC and EPICS applications. Data acquisition can be done as fast as 30 frames/second. At about 4m sample to detector distance, the q range is about 0.002 ~ 0.5 /A from SAXS detector and 0.7 ~ 2.6/A from WAXS detector that is off centered. Data reduction will be done automatically without requiring user interruption. Data viewer and analysis tools are built on Matlab or Igor frame.
12-ID-B uses Linux workstation running SPEC and EPICS applications. Data acquisition can be done as fast as 30 frames/second. At about 4m sample to detector distance, the q range is about 0.002 ~ 0.5 /A from SAXS detector and 0.7 ~ 2.6/A from WAXS detector that is off centered. Data reduction will be done automatically without requiring user interruption. Data viewer and analysis tools are built on Matlab or Igor frame.
Data analysis suite allowing massive in-situ data analysis is available.
Beamline Controls and Data Acquisition
12-ID-B uses Linux workstation running SPEC and EPICS applications. Data acquisition can be done as fast as 30 frames/second. At about 4m sample to detector distance, the q range is about 0.002 ~ 0.5 /A from SAXS detector and 0.7 ~ 2.6/A from WAXS detector that is off centered. Data reduction will be done automatically without requiring user interruption. Data viewer and analysis tools are built on Matlab or Igor frame.
12-ID-B uses Linux workstation running SPEC and EPICS applications. Data acquisition can be done as fast as 30 frames/second. At about 4m sample to detector distance, the q range is about 0.002 ~ 0.5 /A from SAXS detector and 0.7 ~ 2.6/A from WAXS detector that is off centered. Data reduction will be done automatically without requiring user interruption. Data viewer and analysis tools are built on Matlab or Igor frame.
Data analysis suite allowing massive in-situ data analysis is available.