17-BM-B: Rapid Acquisition Powder Diffraction
XSD
Catalysis, Chemistry, GeoScience, Materials Science
Catalysis, Chemistry, GeoScience, Materials Science
17-BM is dedicated to rapid acquisition powder diffraction experiments using an area detector. The versatile set-up can accommodate a wide range of sample environments and is well suited for in situ and operando XRD or PDF measurements, such as battery testing, catalysis, gas loading, electrical catalysis, phase transitions, etc. Visible light Raman Contact "[email protected]" for general beamline inquiries.
Beamline Specifications
Source : Bending Magnet
Monochromator Type : Si(311)
Energy Range : 27-51 keV
Resolution : 5 x 10-3
Flux : 6 x 1010 @27 keV
Beam Size Hxv :
Focused : 500µm x 500µm
Monochromator Type : Si(311)
Energy Range : 27-51 keV
Resolution : 5 x 10-3
Flux : 6 x 1010 @27 keV
Beam Size Hxv :
Focused : 500µm x 500µm
Quick Stats
Current Status
Operational/Accepting General Users
Operational/Accepting General Users
Access Mode
On-site Remote Mail-in
On-site Remote Mail-in
Beamline Contacts
Beamline Techniques
Powder diffraction
X-ray total scattering, pair distribution function (PDF)
Endstations
17-BM-B
monochromatic
monochromatic
Detectors
Varex 4343CT (150 micron pixel size)
X-ray eye
Equipment
Oxford Cryosystems (90-500 K)
Electrical Furnace (RT-1000 C)
Single-channel and Multi-channel Capillary Flow Cells and Mass Flow Controllers
Automatic filling of liquid nitrogen dewars
Diamond Anvil Cells (<10 GPa, DAC expert users only)
User-accessible computers for data processing
Residual Gas Analyzer
Syringe Pump for Gas Loading
Inline RAMAN spectrometer (with prior approval from staff)
Robotic Sample Change System
Block Furnace (RT-400 C)
Electrochemistry cells thru APS E-Chem Lab
Additional Information
Additional Information
https://www.aps.anl.gov/X-ray-Science-Division
https://www.aps.anl.gov/X-ray-Science-Division
Software
EPICS/SPEC for beamline control;
QXRD for data acquisition;
GSAS-II for data processing.
EPICS/SPEC for beamline control;
QXRD for data acquisition;
GSAS-II for data processing.
Beamline Controls and Data Acquisition
EPICS/SPEC for beamline control;
QXRD for data acquisition;
GSAS-II for data processing.
EPICS/SPEC for beamline control;
QXRD for data acquisition;
GSAS-II for data processing.