13-ID-E: Sector 13 X-ray Microprobe

GSECARS
Environmental Science, GeoScience

The 13-ID-E hard x-ray microprobe provides researchers resources for microfocused x-ray fluorescence, absorption spectroscopy, and diffraction analysis at spatial resolution of 0.5 to 2.0 microns

Beamline Specifications
Source Upstream : Undulator 3.3cm - 2.4m or 2.1m length
Source Downstream : Undulator 3.3cm - 2.4m or 2.1m length
Monochromator Type : DCM SI(311)
Energy Range : 4.7-28 keV
Resolution : 3 x 10-5
Flux : 1 x 1012 @10 keV
Beam Size Hxv :
Focused : .5µm x .5µm
Unfocused : .25mm x .25mm

Source Upstream : Undulator 3.3cm - 2.4m or 2.1m length
Source Downstream : Undulator 3.3cm - 2.4m or 2.1m length
Monochromator Type : DCM Si(111)
Energy Range : 2.4-28 keV
Resolution : 1.3 x 10-4
Flux : 6 x 1012 @10 keV
Beam Size Hxv :
Focused : .5µm x .5µm
Unfocused : .25mm x .25mm

Quick Stats
Current Status
Operational/Accepting General Users
Access Mode
On-site Remote
Special Capabilities
Undulator and Si(111) monochromator reach to 2.4 keV for S K-edge sprectroscopy. micro-HERFD (high-resolution fluorescence-detected) XAS with crystal analyzers, and micro-XRF imaging in tomographic mode.
Beamline Contacts
MATTHEW G NEWVILLE
(XAFS, XRF)
Email
ANTONIO LANZIROTTI
(XAFS, XRF)
Email
Beamline Techniques
Micro x-ray absorption fine structure
Microdiffraction
Fluorescence spectroscopy
Microfluorescence
Endstations
IDE
Microflourescence
IDE
Micro X-ray absorption fine structure
IDE
Microdiffraction
Detectors
Mirion 7-element detector with Quantum Xpress Digital Signal Processor (DSP)
Eiger 500K
Eiger 1M
Equipment
Peltier cooled sample stage
Ultraviolet light illuminator
Laboratory facilities including microscopes, fume hood, glove box, etc.
Offline Sample Coordinate and Registration System (OSCAR)
Additional Information
Software
EPICS for instrument and detector control. Python applications for data acquisition and processing.
Beamline Controls and Data Acquisition
EPICS for instrument and detector control. Python applications for data acquisition and processing.