3-ID-B,C,D: NRS
XSD
Chemistry, GeoScience, Life Sciences, Materials Science, Physics
Chemistry, GeoScience, Life Sciences, Materials Science, Physics
Sector 3-ID is operated by the IXN group within X-ray Science Division (XSD). The beamline offers nuclear resonant scattering (NRS) techniques, including nuclear resonant inelastic x-ray scattering (NRIXS) with about 1 meV energy resolution, nuclear forward scattering (NFS) and synchrotron Mossbauer spectroscopy (SMS). An energy-domain Mossbauer spectrometer is under development, will be implemented in the later half of 2025.
Beamline Specifications
Source :
Monochromator Type : Eu HRM
Energy Range : 21.53-21.55 keV
Resolution : 4 x 10-8
Flux : 5 x 108 @21.541 keV
Source :
Monochromator Type : Kr HRM
Energy Range : 9.39-9.42 keV
Resolution : 1 x 10-7
Flux : 5 x 109 @9.404 keV
Source :
Monochromator Type : Dy HRM
Energy Range : 25.64-25.66 keV
Resolution : 2 x 10-8
Flux : 2 x 108 @25.65 keV
Source :
Monochromator Type : Fe HRM
Energy Range : 14.4-14.42 keV
Resolution : 7 x 10-8
Flux : 1 x 1010 @14.413 keV
Beam Size Hxv :
Focused : 2µm x 12µm
Unfocused : 1mm x 1mm
Source :
Monochromator Type : Cryo-cooled Si(111)
Energy Range : 7-27 keV
Resolution : 1.4 x 10-4
Flux : 1.4 x 1014 @14.41 keV
Beam Size Hxv :
Focused : 1µm x 1µm
Unfocused : .7mm x .7mm
Monochromator Type : Eu HRM
Energy Range : 21.53-21.55 keV
Resolution : 4 x 10-8
Flux : 5 x 108 @21.541 keV
Source :
Monochromator Type : Kr HRM
Energy Range : 9.39-9.42 keV
Resolution : 1 x 10-7
Flux : 5 x 109 @9.404 keV
Source :
Monochromator Type : Dy HRM
Energy Range : 25.64-25.66 keV
Resolution : 2 x 10-8
Flux : 2 x 108 @25.65 keV
Source :
Monochromator Type : Fe HRM
Energy Range : 14.4-14.42 keV
Resolution : 7 x 10-8
Flux : 1 x 1010 @14.413 keV
Beam Size Hxv :
Focused : 2µm x 12µm
Unfocused : 1mm x 1mm
Source :
Monochromator Type : Cryo-cooled Si(111)
Energy Range : 7-27 keV
Resolution : 1.4 x 10-4
Flux : 1.4 x 1014 @14.41 keV
Beam Size Hxv :
Focused : 1µm x 1µm
Unfocused : .7mm x .7mm
Quick Stats
Current Status
Operational/Accepting General Users
Operational/Accepting General Users
Access Mode
On-site
On-site
Special Capabilities
High-resolution monochromators: energy bandwidth tunability 9.4 keV 1 meV 20 eV 14.4 keV 1 meV 20 eV 21.6 keV 1.8 meV 20 eV 23.9 keV 0.8 meV 10 eV 25.6 keV 0.6 meV 10 eV microfocusing in 3-ID-B and 3-ID-C; spot size about 1 x 1 micron^2, or 1 x 12 micron^2
High-resolution monochromators: energy bandwidth tunability 9.4 keV 1 meV 20 eV 14.4 keV 1 meV 20 eV 21.6 keV 1.8 meV 20 eV 23.9 keV 0.8 meV 10 eV 25.6 keV 0.6 meV 10 eV microfocusing in 3-ID-B and 3-ID-C; spot size about 1 x 1 micron^2, or 1 x 12 micron^2
Beamline Contacts
Beamline Techniques
Nuclear resonant scattering
Inelastic x-ray scattering (1 meV resolution)
High-pressure diamond anvil cell
Powder diffraction
Endstations
3-ID-B
monochromatic beam station
monochromatic beam station
3-ID-B
nuclear resonant scattering of Eu and Dy
nuclear resonant scattering of Eu and Dy
3-ID-C
monochromatic beam station
monochromatic beam station
3-ID-C
nuclear resonant scattering from Fe under high pressure and/or high/low temperature
nuclear resonant scattering from Fe under high pressure and/or high/low temperature
3-ID-C
Nuclear resonant vibrational spectroscopy on biological and inorganic systems
Nuclear resonant vibrational spectroscopy on biological and inorganic systems
3-ID-D
monochromatic beam station
monochromatic beam station
3-ID-D
nuclear resonant scattering with dual fast shutter system
nuclear resonant scattering with dual fast shutter system
3-ID-D
instrument development
instrument development
Detectors
Avalanche Photo-Diodes
EIGER2 X 500K
PIN diodes
Ion chambers
Equipment
Laser heating system
Online Raman system
Close-cycle liquid He cryostat
Oxford He-bath cryostat with 7-tesla magnet
Oxford He-flow cryostats
Diamond anvil cells for NRS
Additional Information
Additional Information
https://www.aps.anl.gov/Sector-3
https://www.aps.anl.gov/Sector-3
Software
All data aquisition on the beamline is performed on LINUX-based computer using EPICS-based applications running on VME-based electronics. MEDM is used as a graphical interface to display and control various EPICS based devices.
All data aquisition on the beamline is performed on LINUX-based computer using EPICS-based applications running on VME-based electronics. MEDM is used as a graphical interface to display and control various EPICS based devices.
Beamline Controls and Data Acquisition
All data aquisition on the beamline is performed on LINUX-based computer using EPICS-based applications running on VME-based electronics. MEDM is used as a graphical interface to display and control various EPICS based devices.
All data aquisition on the beamline is performed on LINUX-based computer using EPICS-based applications running on VME-based electronics. MEDM is used as a graphical interface to display and control various EPICS based devices.