12-ID-E: High Resolution Small Angle X-ray Scattering
XSD
Chemistry, Materials Science, Physics, Polymer Science
Chemistry, Materials Science, Physics, Polymer Science
The 12-ID-E houses two high-resolution (in reciprocal space) SAXS instruments: a long camera distance pin-hole SAXS and a USAXS instrument. The SAXS instrument is equipped with two area detectors in the 10m long vacuum flight tube for SAXS and WAXS, respectively. With the two detectors, it offers capabilities for simultaneous SAXS and WAXS, Anomalous SAXS and WAXS, and coherent SAXS for x-ray imaging and SAXS/WAXS for scattering. The USAXS instrument is a Bonse-Hart instrument equipped with two area detectors for SAXS and WAXS. In situ experiments are facilitated with ancillary equipment including furnaces, gas and liquid flow systems, stop-flow, high pressure, and burners.
Beamline Specifications
Source :
Monochromator Type : Si (111)
Energy Range : 7-38 keV
Resolution : 1 x 10-4
Flux : 1 x 1012 @12 keV
Beam Size Hxv :
Focused : 5µm x 5µm
Unfocused : 200mm x 100mm
Monochromator Type : Si (111)
Energy Range : 7-38 keV
Resolution : 1 x 10-4
Flux : 1 x 1012 @12 keV
Beam Size Hxv :
Focused : 5µm x 5µm
Unfocused : 200mm x 100mm
Quick Stats
Current Status
Operational/Accepting General Users
Operational/Accepting General Users
Access Mode
On-site
On-site
Special Capabilities
SAXS reciprocal space mapping and coherent SAXS imaging (ptychography).
SAXS reciprocal space mapping and coherent SAXS imaging (ptychography).
Beamline Contacts
Beamline Techniques
Small-angle x-ray scattering
Wide-angle x-ray scattering
Ultra-small-angle x-ray scattering
Coherent x-ray scattering
Anomalous Small Angle X-ray Scattering
Grazing incidence small-angle scattering
Endstations
12-ID-E
USAXS-SAXS-WAXS instrument; 10m long pinhole SAXS instrument
USAXS-SAXS-WAXS instrument; 10m long pinhole SAXS instrument
Detectors
Pilatus2M
Pilatus900K
Equipment
Additional Information
Additional Information
https://www.aps.anl.gov/Sector-12/12-ID-E
https://www.aps.anl.gov/Sector-12/12-ID-E
Software
The SAXS instrument uses windows/linux workstation running SPEC and python GUI for data acquisition. Matlab based software is used for data reduction both in real-time and manually. Data analysis programs, which are for crystal analysis, form/structure factor analysis, background subtraction, integral analysis, and so on, are available at the beamline or downloaded from its web-page. Details of the USAXS instrument are found in https://usaxs.xray.aps.anl.gov/
The SAXS instrument uses windows/linux workstation running SPEC and python GUI for data acquisition. Matlab based software is used for data reduction both in real-time and manually. Data analysis programs, which are for crystal analysis, form/structure factor analysis, background subtraction, integral analysis, and so on, are available at the beamline or downloaded from its web-page. Details of the USAXS instrument are found in https://usaxs.xray.aps.anl.gov/
Beamline Controls and Data Acquisition
The SAXS instrument uses windows/linux workstation running SPEC and python GUI for data acquisition. Matlab based software is used for data reduction both in real-time and manually. Data analysis programs, which are for crystal analysis, form/structure factor analysis, background subtraction, integral analysis, and so on, are available at the beamline or downloaded from its web-page. Details of the USAXS instrument are found in https://usaxs.xray.aps.anl.gov/
The SAXS instrument uses windows/linux workstation running SPEC and python GUI for data acquisition. Matlab based software is used for data reduction both in real-time and manually. Data analysis programs, which are for crystal analysis, form/structure factor analysis, background subtraction, integral analysis, and so on, are available at the beamline or downloaded from its web-page. Details of the USAXS instrument are found in https://usaxs.xray.aps.anl.gov/