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Advanced Photon Source
X-Ray Microscopy and Imaging

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Beamlines and Facilities: Beamline:2-BM

Introduction

The 2-BM beamline offers measurement capabilities for x-ray microtomography, x-ray topography and x-ray microdiffraction. X-ray microtomography and x-ray diffraction instruments are installed on separate optical tables for independent operation with fast switch over time. Optically-coupled high-resolution CCD system is used for microtomography and topography with up to 1 micron spatial resolution. X-ray microdiffraction setup consists of KB microfocussing mirrors (~3 micron minimum spot), four-circle Huber diffractometer, high-precision translation sample stage, two orthogonally-mounted video cameras for viewing sample, fluorescence detector (Si-drift diode) and diffraction detector (a scintillation detector or a CCD).

Three different levels of monochromaticity are available. Conventional monochromatic x-rays from a double-bounced Si (111) crystal monochromator (DCM, D E/E=1E-4), wide band-pass monochromatic x-rays from a double multilayer monochromator (DMM, D E/E=1~4E-2) and pink beam. The available x-ray range is from 5 keV to 30 keV. The lower limit is due to the x-ray windows and the upper limit is due to the critical angle of the x-ray mirror. Two different coatings (Cr and Pt) for the x-ray mirror allow either 20 keV or 30 keV energy cutoff. 

Beamline Scientist:

Francesco De Carlo: decarlo@aps.anl.gov , 630) 252-0148.

Yong S. Chu: ychu@aps.anl.gov , (630) 252-0150

 

Beamline post-doc:

Yuncheng Zhong: yzhong@aps.anl.gov , 630) 252-9748

Xianghui Xiao: xhxio@aps.anl.gov , (630) 252-9621

Konstantin Ignatyev: ignatyev@aps.anl.gov, (630) 252-7881

 

Techniques

•  X-ray Tomography

•  X-ray Topography

•  X-ray microdiffraction

 

Optical Components

Component

Distance from Source

Description

Installed

Filter assembly

23.2 m

8 filters on 2 carriers

05/1996

Hor. and vert. slits

23.5 m

25 µm reproducibility

05/1996

Vert. deflecting mirror

24.9 m

0.15 deg. plane w/ 2 coatings (Cr, Pt)

12/1997

Double multilayer mono.

27.4 m

Unfocussed

05/2000

Double crystal mono

28.8 m

Kohzu, unfocussed

04/1997

Hor. and vert. slits

48.3 m

25 µm reproducibility

02/1997

 

Beamline Configurations

Pink Beam: (2-BM-B)

Beam at sample: 4 x 100 mm 2 (hor x vert), uncollimated

Monochromatic (multilayer): (2-BM-B)

Beam at sample: 4 x 100 mm 2 (hor x vert), E= 0.5-33 keV, dE/E= 10 -2

Monochromatic (crystal): (2-BM-B)

Beam at sample: 4 x 100 mm 2 (hor x vert), E = 2.5-33 keV, dE/E = 10 -4

Detectors

Detector

Manufacturer

Description

Vortex

Radiant technologies

Energy dispersive solid state detector

Coolsnap HQ

Roper, Photometrics

Peltier cooled CCD camera

Quantix 6303e

Roper, Photometrics

Peltier cooled CCD camera (customized)

VersArray:1kb

Roper, Photometrics

Peltier cooled CCD camera

Bicron

 

Scintillator Point Detector

Ion Chambers

 

 

2-BM-B X-ray Optics

KB-Mirrors, University of Chicago design

Parabolic refractive x-ray Be lenses

 

Ancillary Equipment

Micropositioning system

6-circle Huber diffractometer

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