Beamlines and Facilities: Beamline:2-BM
Introduction
The 2-BM beamline offers measurement capabilities for x-ray microtomography, x-ray topography and x-ray microdiffraction. X-ray microtomography and x-ray diffraction instruments are installed on separate optical tables for independent operation with fast switch over time. Optically-coupled high-resolution CCD system is used for microtomography and topography with up to 1 micron spatial resolution. X-ray microdiffraction setup consists of KB microfocussing mirrors (~3 micron minimum spot), four-circle Huber diffractometer, high-precision translation sample stage, two orthogonally-mounted video cameras for viewing sample, fluorescence detector (Si-drift diode) and diffraction detector (a scintillation detector or a CCD).
Three different levels of monochromaticity are available. Conventional monochromatic x-rays from a double-bounced Si (111) crystal monochromator (DCM, D E/E=1E-4), wide band-pass monochromatic x-rays from a double multilayer monochromator (DMM, D E/E=1~4E-2) and pink beam. The available x-ray range is from 5 keV to 30 keV. The lower limit is due to the x-ray windows and the upper limit is due to the critical angle of the x-ray mirror. Two different coatings (Cr and Pt) for the x-ray mirror allow either 20 keV or 30 keV energy cutoff.
Beamline Scientist:
Xianghui Xiao: xhxio@aps.anl.gov , (630) 252-9621
Francesco De Carlo: decarlo@aps.anl.gov , 630) 252-0148.
Beamline post-doc:
Yongshen Pan: pany@aps.anl.gov , (630) 252-5939
Techniques
X-ray Tomography
Optical Components
Component |
Distance from Source |
Description |
Installed |
Filter assembly |
23.2 m |
8 filters on 2 carriers |
05/1996 |
Hor. and vert. slits |
23.5 m |
25 µm reproducibility |
05/1996 |
Vert. deflecting mirror |
24.9 m |
0.15 deg. plane w/ 2 coatings (Cr, Pt) |
12/1997 |
Double multilayer mono. |
27.4 m |
Unfocussed |
05/2000 |
Hor. and vert. slits |
48.3 m |
25 µm reproducibility |
02/1997 |
Beamline Configurations
White Beam: (2-BM-A) |
Beam at sample: 50 x 3 mm 2 (hor x vert), uncollimated |
Pink Beam: (2-BM-B) |
Beam at sample: 50 x 3 mm 2 (hor x vert), uncollimated |
Monochromatic (multilayer): (2-BM-B) |
Beam at sample: 25 x 4 mm 2 (hor x vert), E= 0.5-33 keV, dE/E= 10 -2 |
Detectors
Detector |
Manufacturer |
Description |
Vortex |
Radiant technologies |
Energy dispersive solid state detector |
Coolsnap HQ |
Roper, Photometrics |
Peltier cooled CCD camera |
PCO Edge |
PCO |
sCMOS |
PCO Dimax |
PCO |
CMOS |
Bicron |
|
Scintillator Point Detector |
Ion Chambers |
|
|
2-BM-B X-ray Optics
KB-Mirrors, University of Chicago design
Parabolic refractive x-ray Be lenses
Ancillary Equipment
Micropositioning system
|