Beamline 5-ID-B,C,D: Sector 5 - Insertion Device Beamline

Description

The 5-ID beamline contains three end stations for use by general users.  

 The 5-ID-B station contains a custom 11-detector powder camera formerly stationed at COM-CAT, 32-ID. This system has 11 Si(111) analyzer crystals and operates at an energy of ~ 17.5 keV for high-resolution powder diffraction measurements. The system has a six-position sample changer for capillaries.  

 The 5-ID-C station has two instruments, a kappa diffractometer for in-air or small sample environment cells, and a UHV chamber with MBE and other capabilities. This station has post-monochromator optics for beam conditioning primarily for x-ray standing wave measurements. The UHV system and the post-monochromator optics are only available to general users in a collaborative mode.  

 The 5-ID-D station contains a pinhole small-angle x-ray scattering (SAXS) camera with a maximum sample-to-detector distance of approximately 10 m. Multiple samples can be loaded onto sample wheels and placed inside the vacuum system to produce ultra-low-background SAXS patterns. Simultaneous small- and wide-angle diffraction (SAXS/WAXS) with custom Roper CCD detectors is available on 5-ID-D, including an optional in-vacuum flow cell for solution SAXS/WAXS.    

Supported Techniques

• Powder diffraction
• X-ray standing waves
• X-ray optics development/techniques
• Small-angle x-ray scattering
• Surface diffraction
• X-ray reflectivity
• Wide-angle x-ray scattering

Beamline Controls and Data Acquisition

Linux running custom control code for motors and actuators on all systems. SPEC used to control diffractometers. Vendor-supplied software used to control CCD detectors.

Detectors

• Scintillation detectors
• Mar 165 mm CCD detector
• Microphotonics GEMSTAR 2-D detector
• Roper SAXS/WAXS system
• 11-detector powder camera
• Vortex Silicon Drift Detector

Additional Equipment

• Small kappa 5-circle diffractometer
• Capillary lens
• In-vacuum SAXS setup
• Simultaneous SAXS/WAXS
• Instron servo-hydraulic tensile stage (collaboration only)
• Solution SAXS in-vacuum flow cell

Local Contacts

Beamline Specs

For additional information see:
http://www.dnd.aps.anl.gov/